Microwave assisted extraction of pectin from  dried hull of faba bean

Authors

  • Rafeeya Shams Sam Higginbottom University of Agriculture, Technology and Sciences, Prayagraj, U.P, India Author
  • Dorcus Masih 1 Sam Higginbottom University of Agriculture, Technology and Sciences, Prayagraj, U.P, India Author
  • Ghousia Ashraf Sam Higginbottom University of Agriculture, Technology and Sciences, Prayagraj, U.P, India Author
  • Aamir Hussain Dar Department of Food Technology Islamic University of Science and Technology Awantipora, India Author
  • Qurat ul eain Hyder Rizvi Eternal University, Baru sahib, Himachal Pradesh,India Author

Keywords:

Faba bean hull, equivalent weight, methoxyl content, pectin, degree of esterification

Abstract

 

This study intended to estimate the potential uses of faba bean hull as pectin source for various commercial applications such as gelling, thickening,  stabilization etc. The extraction was carried out at microwave power (160–640 W), time (3–12 min), pH (1.5) and solid: liquid ratio (1:20 g/ml). The  optimal conditions of microwave assisted extraction to yield high pectin from faba bean hull powder (14.86 %) were found to be at pH 1.5, microwave  power of 640 W, extraction time of 9 min, solvent: solid ratio of 1:20 g/ml respectively. The pectin extracted was characterized as high methoxylpectin  with anhydrous acid content and methoxyl content of 51.38% and 4.89% respectively and degree of esterification 54.08%. The extracted pectin  depicted equivalent weight, anhydrouronic acid content and methoxyl content of 746.26%, 51.38% and 4.89% respectively. As little information is  present on extraction of pectin from faba bean hull. The present study revealed that faba bean hull is better and suitable pectin source and considered  to be the potential raw material for various food processing applications.  

References

Aina, A.O., Mustapha, M., Barau, O. A., Mamman, Amina, Z., Hauwa, H., Hauwa, M. S. U. andYagana, B. A. 2012.Extraction and Characterization of Pectin from Peels of Lemon (Citrus limon), Grape Fruit (Citrus paradisi) and Sweet Orange (Citrus sinensis). British Journal of Pharmacology and Toxicology, 3(6): 259-262.

AOAC. 1995. Official Methods of Analysis, 15th ed. Association of Official Analytical Chemists,Washington, DC, USA.

Azad, A.K.M, Ali, M. A., Akter, S., Jiaur, R. M. and Maruf, A. 2014. Isolation and characterization of pectin extracted from lemon pomace during ripening. Journal of Food and Nutrition Sciences,2(2): 30-35.

Barri, T. A. and Shtaya, M.J.Y. 2013. Phenotypic characterization of faba bean (Viciafaba L.) landraces grown in Palestine. Journal of Agricultural Science,5(2):110– 117.

Broomes, J. and Badrie, N. 2010. Effects of Low-Methoxyl Pectin on Physicochemical and Sensory Properties of Reduced Calorie Sorrel/ Roselle (Hibiscus sabdariffa L.) Jams. The Open Food Science Journal,4: 48-55.

Canteri, M. H. G., Scheer, A. P., Ginies, C., Reich, M., Renard, C. M. C. G. and Wosiacki, G.2012. Rheological and macromolecular quality of pectin extracted with nitric acid from passion fruit rind. Journal of Food Process Engineering,35 (5): 800-809.

Castillo-Israel, K. A. T., Baguio, S. F., Diasanta, M. D. B., Lizardo, R. C. M., Dizon, E. I. andMejico, M. I. F. 2015. Extraction and characterization of pectin from Saba banana [Musa ‘saba’ (Musa acuminate × Musa balbisiana)] peel waste: A preliminary study. International Food Research Journal, 22 (1): 202–207.

Constenla, D. and Lozano, J. E. 2003. Kinetic model of pectin demethylation. Latin American Applied Research,33: 91–96.

Endress, H.U. and Christensen, S.H.2009. Pectins. In: Phillips GO, Williams PA (eds) Handbook of hydrocolloids, Edn 2Woodhead Publishing, Cambridge, 274–297.

Eskilsson, C. S. and Björklund, E. 2000. Analytical-scale microwave-assisted extraction. Journal of Chromatography A,902(1): 227–250.

Glinsky, V. V. and Raz, A. 2009. Modified citrus pectin anti-metastatic properties: one bullet, multiple targets. Carbohydrate Research, 344(14): 1788-1791.

Han, W., Meng, Y., Hu, C., Dong, G., Qu, Y., Deng, H. and Guo, Y. 2017. Mathematical model of Ca2+ concentration, pH, pectin concentration and soluble solids (sucrose) on the gelation of low methoxyl pectin. Food Hydrocolloids,66: 37–48.

I.P.P.A. 2014. International Pectin Producers Association Pectin Commercial Production and Pectin in Organic Food Products.

Ismail, N. S. M., Ramli, N., Hani, N. M. and Meon, Z. 2012. Extraction and characterization of pectin from dragon fruit (Hylocereuspolyrhizus) using various extraction conditions. SainsMalaysiana,41 (1): 41-45.

Kalapathy, U. and Proctor, A. 2001. Effect of Acid Extraction and Alcohol Precipitation Conditions on the Yield and Purity of Soy Hull Pectin. Journal Food Chemistry,73:393-396.

Kassegn, H. H., Atsbha, T. W. and Weldeabezgi, L. T. 2018. Effect of germination process on nutrients and phytochemicals contents of faba bean (Viciafaba L.) for weaning food preparation. Cogent Food & Agriculture,4(1): 1545738.

Kastner, H., Kern, K., Wilde, R., Berthold, A., Einhorn-Stoll, U. and Drusch, S. 2014. Structure formation in sugar containing pectin gels – Influence of tartaric acid content (pH) and cooling rate on the gelation of high-methoxylated pectin. Food Chemistry,144: 44–49.

Kjoniksen, A. L., Hiorth, M. and Nystrom, B. 2005. Association under shear flow in aqueous solutions of pectin. EurPolym Journal,41:761–77.

Koh, P. C., Leong, C. M. andNoranizan, M. A. 2014. Microwave-assisted extraction of pectin from jackfruit rinds using different power levels. International Food Research Journal,21 (5): 2091-2097.

Księżak, J., Bojarszczuk, J. and Staniak, M. 2018. Evaluation of the Concentration of Nutrients in the Seeds of Faba Bean (Viciafaba L. major) and PEA (Pisumsativum L.) Depending on Habitat Conditions. Polish Journal of Environmental Studies,27(3): 1133-1143.

Kumar, A. and Chauhan,G. S., 2010. Extraction and characterization of pectin from apple pomace and its evaluation as lipase (steapsin) inhibitor. Carbohydrate Polymers,82: 454–459.

Li, D. Q., Jia, X., Wei, Z. and Liu, Z. Y. 2012. Box–Behnken experimental design for investigation of microwave-assisted extracted sugar beet pulp pectin. Carbohydrate Polymers,88: 342–346.

Li, J., Zu, Y.G., Fu, Y.J., Yang, Y.C., Li, S.M. and Li, Z.N. 2010. Optimization of microwave-assisted extraction of triterpenesaponins from defattedresidue of yellow horn (Xanthocerassorbifolia Bunge.) kernel and evaluation ofits antioxidant activity. Innovative Food Science and Emerging Technologies,11(4): 637–643.

Liang, R. H., Chen, J., Liu, W., Liu, C.M., Yu, W., Yuan, M. andZhou, X. 2012. Extraction, characterization and spontaneous gel-forming property of pectin from creeping fig (Ficuspumila Linn.) seeds. Carbohydrate Polymers,87 (1): 76-83.

Ma, G., Jin, Y., Piao, J., Kok, F., Guusje, B. and Jacobsen, E. 2005. Phytate, calcium, iron, and zinc contents and their molar ratios in foods commonly consumed in China. Journal of Agricultural and Food Chemistry, 53(26):10285-10290.

Maran, P.J., Sivakumar, V., Thirugnanasambandham, K. and Sridhar, R. 2014. Microwave assisted extraction of pectin from waste Citrulluslanatus fruit rinds. Carbohydrate Polymers,101: 786-791.

Minzanova, S., Mironov, V., Arkhipova, D., Khabibullina, A., Mironova, L., Zakirova, Y. and Milyukov, V. 2018. Biological activity and pharmacological application of pectic polysaccharides: A review. Polymers,10(12): 1407.

Noreen, A., Nazli, Z.I.H., Akram, J., Rasul, I., Mansha, A., Yaqoob, N., Iqbal, R., Tabasum, S., Zuber, M. and Zia, K.M. 2017. Pectins functionalized biomaterials; a new viable approach for biomedical applications: A review. International Journal of Biological Macromolecules,101: 254–272.

Ramli, N. and Asmawati, M.S. 2011. Effect of ammonium oxalate and acetic acid at several extraction time and pH on some physicochemical properties of pectin from cocoa husk (Theobroma cacao). African Journal of Food Science,5:790 - 798.

Ruano, P., Delgado, L. L., Picco, S., Villegas, L., Tonelli, F., Merlo, M. E. A. and Masuelli, M. 2019. Extraction and Characterization of PectinsFrom Peels of Criolla Oranges (Citrus sinensis): Experimental Reviews. In Pectins Extraction, Purification, Characterization and Applications. Intech Open.

Sarah, M., Hanum, F., Rizky, M. and Hisham, M.F. 2018. Microwave-assisted extraction of pectin from cocoa peel. In IOP Conference Series: Earth and Environmental Science,122 (1):012079.

Shaha, R.K., Nayagi, Y., Punichelvana, A.P. andAfandi, A. 2013. Optimized extraction condition and characterization of pectin from kaffir lime. Research Journal of Agriculture and Forestry Sciences,1(2): 1-11.

Sundar Raj, A.A., Rubila, S., Jayabalan, R. and Ranganathan, T. V. 2012. A review on pectin: Chemistry due to general properties of pectin and pharmaceutical uses. Scientific reports,1(2): 1-4.

Tamaki, Y., Konishi, T., Fukuta, M. and Tako, M. 2008. Isolation and structural characterization of pectin from endocarp of Citrus depressa. Food Chemistry,107: 352–361.

Triplehorn, C. and Millard, P.S. 2002. A rice-based diet with green banana or pectin reduced diarrhea in infants better than a rice-alone diet. ACP Journal Club,136:67–67.

Wachida, N. andYunianta. 2005. Pectin Extraction from Sweet Orange Skin Review of Maturity Level and Type of Settler. Department of Agricultural Products Technology. BrawijayaUniversity. Malang.

Wang, S., Chen, F., Wu, J., Wang, Z., Liao, X. and Hu, X. 2007. Optimization of pectin extraction assisted by microwave from apple pomace using response surface methodology. Journal of Food Engineering,78: 693-700.

Yadav, S. D., Bankar, N. S., Waghmare, N. N. and Shete, D. C. 2017. Extraction and characterization of pectin from sweet lime. In 4th International Conference on Multidisciplinary Research & Practice, 58-63.

Yan, M.M., Liu, W., Fu, Y.J., Zu, Y.G., Chen, C.Y. and Luo, M. 2010. Optimization of the microwave-assisted extraction process for four main astragalosides in RadixAstragali. Food Chemistry,119: 1663–1670.

Zhang, B., Yang, R. and Liu, C. Z. 2008. Microwave-assisted extraction of chlorogenicacid from flower buds of LonicerajaponicaThunb. Separation and Purification Technology,62:480–483.

Zhao Z.Y., Liang L., Fan X., Yu Z., Hotchkiss A.T., Wilk B.J. and Eliaz I. 2008. The Role of Modified Citrus Pectin as an Effective Chelator of Lead in Children Hospitalized with Toxic Lead Levels. Alternative Therapies in Health and Medicine, 14:34–39.

Published

2020-02-28

How to Cite

Shams, R., Masih, .D., Ashraf, G., Dar, A.H., & Rizvi, Q. ul eain H. (2020). Microwave assisted extraction of pectin from  dried hull of faba bean. Journal of Postharvest Technology, 8(1), 13–22. Retrieved from https://acspublisher.com/journals/index.php/jpht/article/view/15153